Publication background Received29 march 2016Revised19 July 2016Published online16 September 2016Published inissue 8 November 2016

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Electrochemical evaluation is vital skill come teach in chemistry curricula because it is a an important tool in existing high-impact chemistry research. Electrochemistry permits researchers to analysis a range of systems prolonging from molecule to products that incorporate research themes ranging from clean power to substrate activation in organic systems. Specifically, it deserve to reveal information about catalytic efficiency, the role of catalysts, and the nature of chemical reduction and also oxidation (redox) processes. Researchers working in the area the catalysis rely greatly on electrochemistry, utilizing it to identify reliable catalysts and also optimize reaction conditions. This activities experiment begins with an introductory tutorial come electrochemistry through guiding students with the use of several electrochemical approaches using the ferricyanide/ferrocyanide redox pair as a design system. The methods covered in the tutorial incorporate cyclic voltammetry, differential pulse voltammetry, Tafel analysis, and bulk electrolysis. The protocol then uses these techniques to electrocatalysis through identifying and characterizing catalysts because that hydrogen and oxygen generation in the water electrolysis reaction. Electrochemical methods are connected to current chemical research study by concentrating on catalysis in the context of renewable energy, which is a existing societal and curricular imperative. The entire laboratory protocol explained herein is carried out in teams of 2 to three students in a four hour laboratory duration and is suitable for upper-level physical, analytical, or inorganic chemistry.